柔性PANI-SnO2复合薄膜的制备及其对NH3的气敏特性

柔性PANI-SnO2复合薄膜的制备及其对NH3的气敏特性

论文摘要

以苯胺与二氧化锡(SnO2)为前体,通过将原位化学氧化聚合法与静电吸附相结合,在柔性衬底聚酰亚胺(PI)上制备了聚苯胺-二氧化锡(PANI-SnO2)复合薄膜。通过傅里叶红外光谱(FTIR)、扫描电子显微镜(SEM)与X射线衍射(XRD)对复合薄膜的结构与形貌进行表征,证实了PANI-SnO2的成功合成与复合。对其在室温条件下进行了一系列气敏性能测试,结果表明SnO2的添加有效提升了PANI对氨气(NH3)的响应能力;该PANI-SnO2复合薄膜对体积分数为1×10-5~6×10-5的NH3具有良好的灵敏度,此外,该复合薄膜具有良好的重复性与选择性;而且在进行弯折处理后,PANI-SnO2对NH3的响应值并无明显变化。上述结果都表明PANI-SnO2复合薄膜对NH3的检测具有实际应用价值。

论文目录

  • 0 引言
  • 1 实验
  •   1.1 柔性PI衬底的制备及表面处理
  •   1.2 PANI-SnO2复合薄膜的制备
  •   1.3 样品的表征及测试
  • 2 实验结果与分析
  •   2.1 物相结构与表面形貌表征
  •   2.2 气敏性能分析
  • 3 结论
  • 文章来源

    类型: 期刊论文

    作者: 崔艳雷,张铭,李雪伟,王如志

    关键词: 复合薄膜,氨气,气体传感器,柔性衬底,气敏特性

    来源: 微纳电子技术 2019年07期

    年度: 2019

    分类: 信息科技,工程科技Ⅰ辑

    专业: 材料科学

    单位: 北京工业大学材料与工程学院

    基金: 国家自然科学基金资助项目(11774017)

    分类号: TB34

    DOI: 10.13250/j.cnki.wndz.2019.07.010

    页码: 570-574+592

    总页数: 6

    文件大小: 2037K

    下载量: 129

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